Plane-Parallel Microvolume Cells for Studying the Structure of Solutions of Bioorganic Strongly Absorbing and Weakly Scattering Objects at the BioSAX Beamline of Kurchatov Synchrotron Radiation Source

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Abstract

Microvolume cells for studying the structure of solutions by the SAXS method using synchrotron radiation have been designed and created. The cells were tested at the BioMUR station of the Kurchatov synchrotron radiation source. A comparative analysis of two-dimensional small-angle scattering patterns from a standard capillary and from the developed cells has been carried out, which showed a significant improvement in the quality of SAXS experimental data without the need to complicate the data processing procedure when using cells instead of capillaries. The possibility of studying strongly absorbing and weakly scattering samples, as well as the dynamics of SAXS scattering curves for solutions is shown.

About the authors

Andrei E. Sukhanov

NRC “Kurchatov Institute”

Author for correspondence.
Email: sukhanov.ae15@physics.msu.ru
Russian Federation, 59, Leninsky Ave., Moscow, 119333, Russia

Vladimir V. Volkov

NRC “Kurchatov Institute”

Email: volkicras@mail.ru
Russian Federation, 59, Leninsky Ave., Moscow, 119333, Russia

Margarita A. Marchenkova

NRC “Kurchatov Institute”

Email: margaritkaepf@gmail.com
Russian Federation, 59, Leninsky Ave., Moscow, 119333, Russia

Peter V. Konarev

NRC “Kurchatov Institute”

Email: peter_konarev@mail.ru
Russian Federation, 59, Leninsky Ave., Moscow, 119333, Russia

Stanislav Yu. Paul

«Troitsk Research and Development Center» LLC

Email: paul@trdc.com
Russian Federation, 16, Akademik Frank Str., Moscow, Troitsk, 108840, Russia

Georgy S. Peters

NRC “Kurchatov Institute”

Email: georgspeters@gmail.com
Russian Federation, 59, Leninsky Ave., Moscow, 119333, Russia

Yury V. Pisarevsky

NRC “Kurchatov Institute”

Email: yupisarev@yandex.ru
Russian Federation, 59, Leninsky Ave., Moscow, 119333, Russia

Sergei V. Chapek

International Research Institute of Intelligent Materials, SFU

Email: chapek@sfedu.ru
Russian Federation, 178/24, Andrey Sladkov Str., Rostov-on-Don, 344090, Russia

Vladimir A. Shishkov

NRC “Kurchatov Institute”

Email: shiva@crys.ras.ru
Russian Federation, 59, Leninsky Ave., Moscow, 119333, Russia

Alexander V. Soldatov

International Research Institute of Intelligent Materials, SFU

Email: soldatov@sfedu.ru

Professor

Russian Federation, 178/24, Andrey Sladkov Str., Rostov-on-Don, 344090, Russia

Mikhail V. Kovalchuk

NRC “Kurchatov Institute”

Email: koval@crys.ras.ru

RAS Correspondent Member, Professor, President of NRC

Russian Federation, 59, Leninsky Ave., Moscow, 119333, Russia

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Copyright (c) 2024 Sukhanov A.E., Volkov V.V., Marchenkova M.A., Konarev P.V., Paul S.Y., Peters G.S., Pisarevsky Y.V., Chapek S.V., Shishkov V.A., Soldatov A.V., Kovalchuk M.V.

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