Synthesis of gem-dichlorocyclopropane and 1,3-dioxane derivatives from divinylbenzene
- 作者: Raskil’dina G.Z.1, Borisova Y.G.1, Spirikhin L.V.2, Zlotskii S.S.1
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隶属关系:
- Ufa State Petroleum Technological University
- Ufa Federal Research Centre of the Russian Academy of Sciences
- 期: 卷 68, 编号 11 (2019)
- 页面: 2092-2097
- 栏目: Full Articles
- URL: https://ogarev-online.ru/1066-5285/article/view/243532
- DOI: https://doi.org/10.1007/s11172-019-2671-4
- ID: 243532
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详细
The Prins reaction and cyclopropanation of the light fraction obtained by distillation of the technical grade divinylbenzene and consisting of a mixture of 1,3- and 1,4-divinylbenzenes with admixture of 3- and 4-ethylstyrenes were studied. These reactions quantitatively give the corresponding gem-dichlorocyclopropane and 1,3-dioxane benzene derivatives. The structures of the synthesized compounds were confirmed by NMR spectroscopy and mass spectrometry.
作者简介
G. Raskil’dina
Ufa State Petroleum Technological University
编辑信件的主要联系方式.
Email: graskildina444@mail.ru
俄罗斯联邦, 1 ul. Kosmonavtov, Ufa, 450062
Yu. Borisova
Ufa State Petroleum Technological University
Email: spectr@anrb.ru
俄罗斯联邦, 1 ul. Kosmonavtov, Ufa, 450062
L. Spirikhin
Ufa Federal Research Centre of the Russian Academy of Sciences
编辑信件的主要联系方式.
Email: spectr@anrb.ru
俄罗斯联邦, 71 prosp. Oktyabrya, Ufa, Bashkortostan, 450054
S. Zlotskii
Ufa State Petroleum Technological University
Email: spectr@anrb.ru
俄罗斯联邦, 1 ul. Kosmonavtov, Ufa, 450062
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