Synthesis of 1-alkoxy-3-(2-hydroxyethyl)-1-triazene 2-oxides

G. A. Smirnov; P. B. Gordeev; S. V. Nikitin; G. V. Pokhvisneva; T. V. Ternikova; O. A. Luk’yanov

doi:10.1007/s11172-016-1630-6

Synthesis of 1-alkoxy-3-(2-hydroxyethyl)-1-triazene 2-oxides

Authors: Smirnov G.A.¹, Gordeev P.B.¹, Nikitin S.V.¹, Pokhvisneva G.V.¹, Ternikova T.V.¹, Luk’yanov O.A.¹
Affiliations:
1. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences
Issue: Vol 65, No 11 (2016)
Pages: 2644-2649
Section: Full Articles
URL: https://ogarev-online.ru/1066-5285/article/view/239309
DOI: https://doi.org/10.1007/s11172-016-1630-6
ID: 239309

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Abstract

Synthetic procedure to access the first representatives of a new series of 3-monosubstitued functional derivatives of 1-alkoxy-1-triazene 2-oxides, i.e., 1-alkoxy-3-(2-hydroxyethyl)- and 1-alkoxy-3-(2-acetoxyethyl)-1-triazene 2-oxides, were elaborated. 1-Alkoxy-3,3-bis(2-hydroxyethyl)-1-triazene 2-oxides were used to derive 3-(2-acetoxyethyl)-, 3-(2-bromoethyl)- and 3-(2-cyanoethyl)substituted 1-alkoxy-3-(2-acetoxyethyl)-1-triazene 2-oxides.