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Vol 48, No 7 (2018)

Article

Inspection of the Metal Microstructure in Laser-Surfaced Rollers

Belonosov A.V., Chikova O.A., Zaitseva N.A.

Abstract

The microstructure and crystalline structure of laser-surfaced 9Kh2MF and 8Kh3SMFA steel samples are studied. Samples are taken from the working rollers of the reversible rolling mill at PAO Uralmashzavod. Sealing of surface cracks in the rollers by means of a laser is regarded as an effective repair method in small-scale production. The goal of the research is to monitor the quality of laser-surfaced steel components. The inspection focuses on metallurgical defects (nonmetallic inclusions, gaps, regions with nonuniform chemical composition) in the surfacing zone and the surrounding thermal influence zone. An ultrasound method is employed. Metallographic study of the microstructure and crystalline structure of laser-surfaced steel samples is necessary in order to develop an ultrasonic monitoring method. Metallurgical defects in steel are mainly found by means of a scanning electron microscope capable of X-ray spectral microanalysis (EDS analysis) and electron back-scattering diffraction (EBSD analysis). The present work employs a Carl Zeiss Auriga Crossbeam scanning electron microscope with EDS analysis of the surface’s elemental composition and EBSD analysis of the surface’s crystalline structure. The metallographic data for the laser-surfaced steel samples from the rollers reveal metallurgical defects along the boundary of the surfacing zone. The microheterogeneities measure 10–50 and 1–3 μm for 9Kh2MF and 8Kh3SMFA steel, respectively. The elements present include Mn, Si, and O for 9Kh2MF steel and Mn, Cr, and Mo for 8Kh3SMFA steel. The surface metal is found to be less textured than the basic metal and has more uniform acoustic characteristics. That must be taken into account in ultrasound monitoring of laser-surfaced steel components. In the ultrasound monitoring of laser-surfaced working rollers, signal recording with reflectivity equivalent to a flat-bottomed hole of 1.5-mm diameter is recommended.

Steel in Translation. 2018;48(7):403-410
pages 403-410 views

SHS Technology for Composite Ferroalloys. 2. Synthesis of Ferrosilicon Nitride and Ferrotitanium Boride

Ziatdinov M.K., Shatokhin I.M., Leont’ev L.I.

Abstract

The combustion of ferrosilicon in nitrogen is very similar to the combustion of metallic silicon. With increase in silicon content in the initial ferrosilicon, its reaction rate with nitrogen increases, as is clear from the considerably more vigorous combustion. The nitrogen concentration in the combustion products increases here. Over the whole range of initial parameters (nitrogen pressure, grain size of the powder, batch composition), the combustion products consist mainly of β-Si3N4. No large quantity of α-Si3N4 is observed. In practice, FS75 and FS90 ferrosilicon is optimal for refractory production, while FS65 and FS75 ferrosilicon, with lower impurity content, is best for the production of components used in steel production. The introduction of iron in the Ti–B system (Tad = 3190 K) considerably restricts the combustion concentration range. A mixture with 16.9% B burns in a narrow Ti:B concentration range close to 0.86. In combustion of the Fe–B + Ti mixture, increase in the initial temperature considerably expands the concentration range for synthesis. In all cases, increase in the initial temperature considerably boosts the combustion rate. Heating to T0 ≥ 300°C permits the use of mixtures with titanium powder containing larger grains (rme.Ti ≥ 0.4 mm) in self-propagating high-temperature synthesis (SHS). A wide range of B:Ti ratios may be used. The combustion of such mixtures permits the production of an alloy with 6–14% B and 30–60% Ti. Specialized industrial equipment has been constructed: a series of SHS reactors with working volumes of 0.06, 0.15, and 0.3 m3, permitting the large-scale production of materials based on refractory inorganic compounds for use in metallurgy. The industrial production of composites based on oxygen-free compounds by self-propagating hightemperature synthesis has been introduced.

Steel in Translation. 2018;48(7):411-418
pages 411-418 views

Factors Affecting the Life of Steel Grating Bars in Roasting Cars

Ivanov D.I., Kozhukhov A.A., Sklyar V.A.

Abstract

To understand the factors affecting the working life of 40Kh24N12SL steel grating bars in roasting cars, we compare data regarding the grating bars after operation with the results of simulating their operating conditions. The results obtained by finite-element modeling are highly reliable. In modeling, the maximum possible number of boundary conditions is specified on the basis of the data regarding the grating bars already obtained and literature data. Modeling shows that a considerable temperature is formed over the part’s cross section, with local heating zones. The heating is predictable and is associated with the supply of coolant to the working zone in the course of operation. Over time, zones with large internal stress and strain are formed locally in the part. The appearance of these zones depends strongly on the presence of structural inhomogenities of the part and is thought to be associated with the geometric complexity of the casting. In the presence of shrinkage cavities, all of the stress and strain values increase sharply, especially at local maxima. The distribution of the local zones with high stress and strain remains practically unchanged in the presence of shrinkage cavities. Analysis of the position of the zones with high stress and strain sheds light on the grating bar failure by cracking in the course of operation. The presence of shrinkage cavities in the metal is found to be a major cause of the buckling, cracking, and fracture of 40Kh24N12SL steel grating bars in roasting cars. Simulation of the operating conditions permits explanation of the defect formation in the grating bars in accordance with observational data.

Steel in Translation. 2018;48(7):419-423
pages 419-423 views

Effectiveness of Blind Feeders in Steel Casting

Fedosov A.V., Chumachenko G.V., Khodarev M.A., Golomeev V.V.

Abstract

Existing methods of decreasing feeder size are briefly reviewed, with an account of their advantages and disadvantages. The applicability of methods of optimizing the feeder shape so as to increase the useful volume of the casting is identified. The actual position of shrinkage defects in feeders of different structure is considered. The position and shape of shrinkage cavities are considered as a function of the shape of the feeder’s upper section. Four groups of feeders are distinguished, and their effectiveness is compared. Mathematical modeling is proposed to better understand the formation of shrinkage cavities in feeders with different designs of their upper section and to assess their effectiveness. Mathematical modeling permits analysis of the external factors affecting the thermal processes in the mold, which is difficult in casting practice. SolidCast software is used. The initial and boundary conditions in modeling are identical for feeders of all types. The predictions regarding the shrinkage defects are expressed as isosurfaces, whose dimensions may be used to assess feeder effectiveness. The modeling results are used to develop an approach to assessing the thermal efficiency of feeders of different types. The estimates are based on the position of the shrinkage defect within the feeder. As an example, the effectiveness of feeders of the same size but with different configurations of the upper section is calculated. The proposed efficiency index is in good agreement with the geometric modulus (the ratio of the feeder’s volume to its surface area). Increase in the feeder’s modulus increases its thermal efficiency. The introduction of a notch increases the feeder’s efficiency. Analysis of isothermal lines in the longitudinal section of the feeder permits description of the thermal operation of the notch and its influence on the position of the shrinkage cavity. Recommendations are made for increasing the casting yield by redesigning the feeder’s upper section. The casting yield may be increased by 4%, with accompanying decrease in the rejection rate of the castings, thanks to optimization of the feeder’s upper section.

Steel in Translation. 2018;48(7):424-429
pages 424-429 views

Quality of Rolled Steel for Cold Bulk Stamping

Filippov A.A., Pachurin G.V., Kuz’min N.A., Matveev Y.I., Deev V.B.

Abstract

Metal products obtained from rolled blanks by cold upsetting are used in every branch of manufacturing. The quality of such components is assessed in terms of the required chemical composition and the plasticity, the consistency of the mechanical characteristics over the whole length, and the lack of internal and surface defects. If such metal components are to be competitive, all the steps in the production chain must be optimized: from smelting of the steel to cold upsetting of the product. In attempting to minimize costs and ensure the required quality, it is important to ensure safety and to decrease energy and labor costs in manufacturing. In this chain, the preparation of the material for cold bulk stamping is a key step. The high-strength fasteners obtained by cold upsetting are most often made of chrome steel. Recently, alternative boron-bearing steels have been actively introduced. However, their thermal hardening in quenching is unstable because boron oxides and nitrides may be formed, with decrease in their hardenability. In addition, chrome steels are 12–16% cheaper, as a rule. Also, since foreign supplies of boron steels are associated with additional costs, fasteners made of boron steels are even more expensive. That is a further impetus to using chrome steels. In the present work, we obtain standard mechanical characteristics and failure criteria for 40Kh steel components patented in a saltpeter bath at different temperatures, with subsequent drawing. The optimal preparation of the rolled steel in terms of its structural and mechanical characteristics after cold bulk stamping is determined: patenting (in a saltpeter bath at 400°C) and drawing (with 5–10% reduction). Such treatment yields products of the required quality and is preferable to the existing technology.

Steel in Translation. 2018;48(7):430-434
pages 430-434 views

Processing Ash and Slag Wastes from Thermal Power Stations. Part 2

Agapov E.A., Erokhov T.V., Kozlova O.N., Podgorodetskii G.S., Gorbunov V.B.

Abstract

For existing coal-fired power plants, current methods of utilizing ash and slag waste may be considered in addressing new environmental and economic risks. However, for new power sources, environmental considerations are much more important in selecting the coal-combustion technology. Technology based on a circulating fluidized bed is sometimes cited as the most promising approach to environmentally sound coal combustion. It permits significant decrease in emissions of sulfur and nitrogen oxides beyond the boiler, but is of no help in processing ash and slag waste. For waste disposal, a different approach is recommended for new plants or the upgrading of coal-fired plants: instead of coal combustion in a gas flux or a fluidized bed, combustion in bubbling slag melt. Such methods are described. The basic characteristics of pulverized-coal combustion and combustion in slag melt are compared. Two basic approaches to the development of coal-based power generation are proposed: coal combustion with supercritical steam parameters; and gas generation with a hybrid (steam + gas) power-generating cycle based on gasification of solid fuels. The electrical efficiency of steam-based plants may be increased from 30–36 to 44–45% with supercritical steam parameters; and to 50–55% when using a hybrid steam–gas cycle. The proposed industrial system for coal gasification in slag melt increases the overall electrical efficiency. The environmental and economic efficiency of carbon gasification is demonstrated. It is simple to produce components from slag by casting. The cast slag–coal components are of considerably higher quality than analogous cement–sand components with added fly ash. The ease of switching from one type of casting to another permits rapid response to market demand.

Steel in Translation. 2018;48(7):435-440
pages 435-440 views

Structure and Properties of Carbon Steel Wire in Drawing

Chukin M.V., Polyakova M.A., Pivovarova K.G., Efimova Y.Y., Gulin A.E.

Abstract

A method of continuous deformational nanostructuring of wire is described. In the method, a continuously moving wire is subjected simultaneously to tensile deformation in drawing, flexural deformation on passing through a roller system, and torsional deformation. This combination permits wide variation in its mechanical properties, ensuring both high strength and plasticity. The benefits of such deformation are the use of a tool already employed in the production of metal components; compatibility with the speeds of coarse and moderate wire drawing; and simplicity of the equipment. Laboratory apparatus for this method is described. Carbon steel 50 wire is selected for investigation, since it in great demand. The chemical composition and mechanical properties of the wire in the initial state are described. Experiments are conducted to investigate the effectiveness of the proposed differential nanostructuring in producing ultrafine-grain structure in the wire. The deformation conditions of the wire are described, as well as the drawing process. The transverse and longitudinal microstructure of the carbon steel 50 wire at the surface and in the center after different types of deformational treatment is investigated. In the experiments, the influence of the type of deformational treatment on the microstructure of the steel and its anisotropy over the wire cross section is established. The compliance of the wire’s mechanical properties with current standards is verified. After all types of treatment, its mechanical properties are consistent with State Standard GOST 17305–91. Metallographic data and mechanical test results after combined deformational treatment indicate that such combinations of deformation provide a promising approach to creating ultrafine-grain structure in carbon wire.

Steel in Translation. 2018;48(7):441-445
pages 441-445 views

Solid-Fuel Combustion in the Sintering of Siderite Ore

Yur’ev B.P., Dudko V.A.

Abstract

Two technologies are considered for the preparation of solid fuel used in sintering: crushing with portions of roasted siderite ore whose strength is less than that of the fuel; or crushing of the fuel alone and subsequent mixing with the ore portions. On the basis of derivatographic data, kinetic equations are written for the high-temperature combustion of coke fines in a fuel–ore mixture obtained by the two methods. The most flammable fuel fraction in sintering is established. The results indicate that crushing of the fuel mixed with weaker additives is more effective in terms of decreasing the content of fines in the fuel and hence intensifying the combustion of large pieces.

Steel in Translation. 2018;48(7):446-450
pages 446-450 views

Boundary-Condition Selection in Simulating the Secondary-Cooling Zone in the Continuous-Casting Machine

Dozhdikov V.I., Vasyutin A.Y., Cherkasov N.V.

Abstract

Methods of specifying the boundary conditions in the secondary-cooling zone of the continuous-casting machine are compared in simulating slab solidification. Experimental data are used to assess the correctness of the models. The results of simulation are different when using the mean heat-transfer coefficient for the section of the continuous-casting machine and the local heat-transfer coefficients for the zones with and without coolant. The modeling results are compared with experimental data for the surface temperature of the continuous-cast ingot at the center of its broad face.

Steel in Translation. 2018;48(7):451-453
pages 451-453 views

Frictional-Stress Distribution in the Deformation Zone on Cold Rolling

Kozhevnikova I.A., Bolobanova N.L., Yusupov V.S., Kozhevnikov A.V., Kroitor E.N.

Abstract

The influence of the operating conditions on the frictional-stress distribution in the deformation zone on cold rolling is studied numerically on the basis of DEFORM-2D software. By adjusting the rolling conditions so as to regulate the tangential stress, the surface contamination of the strip may be decreased.

Steel in Translation. 2018;48(7):454-457
pages 454-457 views

Macro- and Micromechanics of Pearlitic-Steel Deformation in Multistage Wire Production

Konstantinov D.V., Korchunov A.G., Zaitseva M.V., Shiryaev O.P., Emaleeva D.G.

Abstract

Ninefold drawing of pearlitic steel wire is investigated. On the basis of multiscale computer models, the behavior of pearlite colonies at the surface of the wire and in its central layer is analyzed. The key factors are the orientation of the cementite lamellae relative to the drawing axis, the interlamellae distance, and the shape of the cementite inclusions. On the basis of finite-element models, the laws governing the reorientation of the pearlite colonies, change in shape and size of the cementite lamellae, and localization of the deformation in the ferrite are determined. The model results are verified by means of metallographic results and industrial experiments.

Steel in Translation. 2018;48(7):458-462
pages 458-462 views

Influence of Heat Treatment on the Microstructure and Low-Temperature Performance of Low-Carbon Steel

Bagmet O.A., Sokolova M.Y., Naumenko V.V.

Abstract

In the present work, 20L and 20GL steels are investigated with a view to increase in their impact strength at negative temperatures, by adjusting the structural state in final heat treatment of valve and pipeline components. Stable impact strength KCV may be established in 20L steel at –40°C and in 20GL steel at ‒60°C by three-stage heat treatment: double quenching in water and subsequent high tempering. The other three heat treatments considered proved ineffective. The greater strength of 20GL steel components in comparison with 20L steel components may be attributed to its finer structure and greater bulk content of acicular α phase, on account of the higher content of manganese, which deters the ferrite transformation of austenite.

Steel in Translation. 2018;48(7):463-471
pages 463-471 views

Evolution of the Defect Structure of Pearlitic Steel in Cold Deformation

Parusov E.V., Sukhomlin G.D., Gubenko S.I., Sychkov A.B., Denisenko A.I., Kamalova G.Y.

Abstract

A method of microdiffraction analysis is developed in order to determine the defect structure of pearlitic steels during cold plastic deformation. The total reduction in the drawing of C86D steel coil is shown to affect the azimuthal blurring of the subreflexes in the microdiffraction pattern and the distortion of the plates in the pearlite colony.

Steel in Translation. 2018;48(7):472-477
pages 472-477 views

Production of Amorphous Alloys for Cybernetic Circuits

Molotilov B.V., Eremin G.N., Shestakova T.A.

Abstract

The ways in which the manufacturing conditions affect the magnetic (domain) structure of amorphous alloy strip produced on cooled disks are studied. On that basis, the physical properties of the alloys may be optimized for their intended use.

Steel in Translation. 2018;48(7):478-481
pages 478-481 views