Effect of Template Structure on the Zeolite ZSM-12 Crystallization Process Characteristics
- Authors: Kulikov L.A.1, Tsaplin D.E.1, Knyazeva M.I.2, Levin I.S.2, Kardashev S.V.1, Filippova T.Y.1, Maksimov A.L.1,2, Karakhanov E.A.1
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Affiliations:
- Faculty of Chemistry, Moscow State University
- Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences
- Issue: Vol 59, No Suppl 1 (2019)
- Pages: S60-S65
- Section: Article
- URL: https://ogarev-online.ru/0965-5441/article/view/181039
- DOI: https://doi.org/10.1134/S0965544119130097
- ID: 181039
Cite item
Abstract
Characteristics of zeolite ZSM-12 crystallization using methyltriethylammonium chloride and N,N-dimethyl-N-ethyl(monoethanol)ammonium bromide as templates have been studied. The materials have been characterized by X-ray diffraction analysis, scanning electron microscopy, X-ray fluorescence analysis, low-temperature nitrogen adsorption–desorption, temperature-programmed desorption of ammonia, and solid-state 27Al nuclear magnetic resonance spectroscopy. It has been shown that dimethylethylethanolammonium bromide inhibits crystal growth along the a and c planes and thereby contributes to crystal growth only in the direction of the b axis, which, in turn, leads to lower surface area and acidity of the sample than the respective parameters of the zeolite synthesized using methyltriethylammonium chloride.
Keywords
About the authors
L. A. Kulikov
Faculty of Chemistry, Moscow State University
Author for correspondence.
Email: mailforleonid@mail.ru
Russian Federation, Moscow, 119991
D. E. Tsaplin
Faculty of Chemistry, Moscow State University
Email: mailforleonid@mail.ru
Russian Federation, Moscow, 119991
M. I. Knyazeva
Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences
Email: mailforleonid@mail.ru
Russian Federation, Moscow, 119991
I. S. Levin
Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences
Email: mailforleonid@mail.ru
Russian Federation, Moscow, 119991
S. V. Kardashev
Faculty of Chemistry, Moscow State University
Email: mailforleonid@mail.ru
Russian Federation, Moscow, 119991
T. Yu. Filippova
Faculty of Chemistry, Moscow State University
Email: mailforleonid@mail.ru
Russian Federation, Moscow, 119991
A. L. Maksimov
Faculty of Chemistry, Moscow State University; Topchiev Institute of Petrochemical Synthesis, Russian Academy of Sciences
Email: mailforleonid@mail.ru
Russian Federation, Moscow, 119991; Moscow, 119991
E. A. Karakhanov
Faculty of Chemistry, Moscow State University
Email: mailforleonid@mail.ru
Russian Federation, Moscow, 119991
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