Synthesis and structural features of Co(II) compounds with 3-arylidene-1-pyrroline derivatives and monocarboxylic acids anions

Мұқаба

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат Ашық рұқсат
Рұқсат жабық Рұқсат берілді
Рұқсат жабық Тек жазылушылар үшін

Аннотация

A series of acetate and trifluoroacetate compounds of cobalt(II) with derivatives of 3-arylidene-1-pyrrolines (X-L; X = Cl, OH) as N-donor ligands was synthesized. Varying the synthesis and crystallization conditions made it possible to obtain coordination compounds of various compositions and structures: a tetranuclear complex based on a cubane fragment {Co4(OH)4}4– — [Co4(OH)4(Cl–L)4(OAc)4] (I), a 1D-polymer complex [Co(H2O)(Cl–L)2(CF3COO)1.167(OAc)0.833]n (II) or a molecular complex [Co(OH–L)2(OAc)2] (III). The synthesized compounds were characterized by X-ray diffraction, IR spectroscopy and CHN analysis. The structure and crystal packing of the obtained complexes were analyzed in detail, the main structure-forming non-covalent interactions in crystals were identified.

Авторлар туралы

Yu. Voronina

N. S. Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Хат алмасуға жауапты Автор.
Email: juliavoronina@mail.ru
Moscow, Russia

O. Zvereva

N. S. Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences; A. N. Nesmeyanov Institute of Organoelement Compounds of the Russian Academy of Sciences

Email: juliavoronina@mail.ru
Moscow, Russia; Moscow, Russia

M. Shmelev

N. S. Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: juliavoronina@mail.ru
Moscow, Russia

E. Zorina-Tikhonova

N. S. Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: juliavoronina@mail.ru
Moscow, Russia

A. Rogachev

MIREA — Russian Technological University

Email: juliavoronina@mail.ru
Moscow, Russia

A. Sidorov

N. S. Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: juliavoronina@mail.ru
Moscow, Russia

I. Eremenko

N. S. Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: juliavoronina@mail.ru
Moscow, Russia

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