Email this article Validation of a Method for Assay of Sulfur Hexafluoride in a New Contrast Agent by Gas Chromatography
- Authors: Krivoshchekov S.V.1,2, Lar’kina M.S.1, Vlasov S.S.1,2, Drygunova L.A.1,2, Gur’ev A.M.1, Belousov M.V.1, Yusubov M.S.1,2
-
Affiliations:
- Siberian State Medical University, Russian Ministry of Health
- National Research Tomsk Polytechnic University
- Issue: Vol 51, No 3 (2017)
- Pages: 222-225
- Section: Article
- URL: https://ogarev-online.ru/0091-150X/article/view/244540
- DOI: https://doi.org/10.1007/s11094-017-1586-3
- ID: 244540
Cite item
Open Access
Access granted
Subscription Access
Abstract
Amethod for assaying sulfur hexafluoride in a new contrast agent by gas chromatography is described. Detection was with an electron capture detector (ECD). Sulfur hexafluoride was extracted from samples using heptane as the solvent. The method was validated in terms of the following parameters: specificity, linearity, correctness, stability, and inter- and intralaboratory precision.
Keywords
About the authors
S. V. Krivoshchekov
Siberian State Medical University, Russian Ministry of Health; National Research Tomsk Polytechnic University
Email: marialarkina@mail.ru
Russian Federation, 2 Moskovskii Tract, Tomsk, 634040; 30 Lenin Prospekt, Tomsk, 634050
M. S. Lar’kina
Siberian State Medical University, Russian Ministry of Health
Author for correspondence.
Email: marialarkina@mail.ru
Russian Federation, 2 Moskovskii Tract, Tomsk, 634040
S. S. Vlasov
Siberian State Medical University, Russian Ministry of Health; National Research Tomsk Polytechnic University
Email: marialarkina@mail.ru
Russian Federation, 2 Moskovskii Tract, Tomsk, 634040; 30 Lenin Prospekt, Tomsk, 634050
L. A. Drygunova
Siberian State Medical University, Russian Ministry of Health; National Research Tomsk Polytechnic University
Email: marialarkina@mail.ru
Russian Federation, 2 Moskovskii Tract, Tomsk, 634040; 30 Lenin Prospekt, Tomsk, 634050
A. M. Gur’ev
Siberian State Medical University, Russian Ministry of Health
Email: marialarkina@mail.ru
Russian Federation, 2 Moskovskii Tract, Tomsk, 634040
M. V. Belousov
Siberian State Medical University, Russian Ministry of Health
Email: marialarkina@mail.ru
Russian Federation, 2 Moskovskii Tract, Tomsk, 634040
M. S. Yusubov
Siberian State Medical University, Russian Ministry of Health; National Research Tomsk Polytechnic University
Email: marialarkina@mail.ru
Russian Federation, 2 Moskovskii Tract, Tomsk, 634040; 30 Lenin Prospekt, Tomsk, 634050
Supplementary files
