Key operations for production of laboratory cryostats for photodetectors

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Abstract

BACKGROUND: A microcryogenic system for cryostatting the photosensitive matrix is a main component of the photodetector cryomodule. This paper discusses a passive cryostatting system for laboratory photodetectors used in research to expand the capabilities of cooled infrared systems. The passive microcryogenic system is a nitrogen filling high-vacuum Dewar cryostat. Its most common issue is the loss of thermal insulation properties due to atmospheric air leakage.

AIM: This study aimed to minimize atmospheric air leakage into the evacuated volume of a laboratory cryostat to extend its service life.

METHODS: The study is an experimental correlation study based on monitoring the cryostat service life to find a solution increasing it by reducing the amount of leakage and follow-up leak monitoring. The study object is a high-vacuum cryostat based on a brazed Dewar container. The study was conducted over a period of two weeks. We selected a soldering technique, conducted an experiment with follow-up leak monitoring and assessment of the cryostat operating life.

RESULTS: The findings are shown in photographs of different soldering techniques. The welding seam produced with PSr8KTsN solder shows no erosion of the base metal with the minimum chemical compound layer and no cracks.

CONCLUSION: Gaseous helium leakage rate into the vacuum cavity of the laboratory cryostat was 3.2 · 10-13 Pa · m3/s, which corresponds to a continuous operation time of the product of at least 5 years under laboratory operating conditions.

About the authors

Andrew V. Samvelov

Limited Liability Company “Cryonex Scientific and Technical Center”

Author for correspondence.
Email: samv-andrej@yandex.ru
ORCID iD: 0000-0002-5840-7626
SPIN-code: 9932-6353

Cand. Sci. (Engineering)

Russian Federation, Moscow

Alexander S. Moskalenko

Limited Liability Company “Cryonex Scientific and Technical Center”

Email: a-moskalenko@inbox.ru
ORCID iD: 0000-0002-1657-5015
SPIN-code: 5571-1233
Russian Federation, Moscow

Natalia E. Shishova

Bauman Moscow State Technical University

Email: natalia-shishova@gmail.com
ORCID iD: 0009-0005-2763-7997
SPIN-code: 3133-1035

Cand. Sci. (Engineering)

Russian Federation, Moscow

References

  1. Khryapin VE. Soldering Iron Handbook. Moscow: Mashinostroenie; 1981. (In Russ.)
  2. Arkharov AM, Arkharov IA, Belyakov VP, et al. Cryogenic systems. Moscow: Mashinostroenie; 1987. (In Russ.)
  3. Baranov AYu, Sokolova EV. Storage and transportation of cryogenic liquids. Part 1: Study guide. St. Petersburg: ITMO University; 2017. (In Russ.) EDN: LPKPVM
  4. Popov VM. Heat transfer in the contact zone of detachable and non-removable joints. Moscow: Energiya; 1971. (In Russ) EDN: RELYGR
  5. Grezin AK, Zinoviev VS. Microcryogenic technology. Moscow: Mashinostroenie; 1977. (In Russ.)
  6. Kitaev AM, Gubin AI. Welding and soldering of thin-walled pipelines. Moscow: Mashinostroenie; 1972. (In Russ.)
  7. Deniz EK, Bredenbeck ED. An automatic liquid nitrogen refilling system for small (detector) Dewar vessels Review of Scientific Instruments 89; 116101; 2018.
  8. Willems D, Garcia S, Arts R, et al. Theoretical and experimental analysis of Dewar thermal properties. In: SPIE 11002. Infrared Technology and Applications XLV; 1100208. SPIE; 2019.

Supplementary files

Supplementary Files
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1. JATS XML
2. Fig. 1. Dimensional drawing of a laboratory cryostat. 1, viewing optical window; 2, aperture; 3, IR photodetector seat; 4, metal-ceramic unit with contacts; 5, inner vessel; 6, outer vessel; 7, thermal supports; 8, neck; 9, exhaust tube; 10, getter.

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3. Fig. 2. Sections of seams of KhN70VMTYu steel sheets welded using various solders. a, PSr8KTsN solder; b, Cd-5Ag solder; c, Pb-Ag2.5-Cu solder.

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