Three-step synthesis of Pd0/TiO2


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A simplifi ed procedure for the synthesis of Pd0/TiO2 xerogel has been developed, which includes the following steps: hydrolysis of tetrabutoxytitanium from its mixture with a palladium salt in an acetic acid atmosphere, drying and calcining the material at 860 °C. Palladium in the calcined xerogel is present in the form of spherical particles, titanium dioxide — as rutile aggregates.

Sobre autores

A. Shishmakov

I. Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences

Email: mikushina@ios.uran.ru
Rússia, 22/20 ul. S. Kovalevskoi, Ekaterinburg, 620990

Yu. Mikushina

I. Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences

Autor responsável pela correspondência
Email: mikushina@ios.uran.ru
Rússia, 22/20 ul. S. Kovalevskoi, Ekaterinburg, 620990

L. Petrov

I. Ya. Postovsky Institute of Organic Synthesis, Ural Branch of the Russian Academy of Sciences

Email: mikushina@ios.uran.ru
Rússia, 22/20 ul. S. Kovalevskoi, Ekaterinburg, 620990

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