SOLID SOLUTIONS AND PHASE EQUILIBRIA IN THE NiO-ZnO-SiO2 SYSTEM IN THE SUBSOLIDUS REGION

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Resumo

Substitution solid solutions Zn2-2xNi2xSiO4 (willemite structure), Ni2-2yZn2ySiO4 (olivine structure) and Ni1-zZnzO (rock salt structure) were synthesized by solid-phase synthesis in air, and their extents were determined. Phase equilibria in the NiO-ZnO-SiO2 system in the subsolidus region were revealed based on the phase composition of the binary systems NiO-ZnO, ZnO-SiO2, NiO-SiO2, control points and parameters of the unit cells of solid solutions. It has been established that the ternary system NiO-ZnO-SiO2 is divided by conodes into seven elementary fields. Phase equilibria in the NiO-ZnO-SiO2 system is determined by the quasi-binary equilibrium of the boundary compositions of the Zn2-2xNi2xSiO4 (x = 0.10) and Ni2-2yZn2ySiO4 (y = 0.25) solid solutions and the conodes connecting these compositions with the Ni1-zZnzO solid solution, as well as the conode connecting the boundary composition of the Ni1-zZnzO (z = 0.4) solid solution with Zn2SiO4.

Sobre autores

E. Dobrynenko

Institute of Solid State Chemistry, Ural Branch of Russian Academy of Sciences

Email: natalzay@yandex.ru
Ekaterinburg, Russia

N. Zaitseva

Institute of Solid State Chemistry, Ural Branch of Russian Academy of Sciences; Ural State Mining University

Ekaterinburg, Russia

R. Samigullina

Institute of Solid State Chemistry, Ural Branch of Russian Academy of Sciences

Ekaterinburg, Russia

T. Krasnenko

Institute of Solid State Chemistry, Ural Branch of Russian Academy of Sciences

Ekaterinburg, Russia

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